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Single Laboratory Validation Report for Total Amino Acids by UHPLC-UV in Infant Formulas and Adult Nutritionals - APPENDICES

Jaudzems, Lahrichi, and Fuerer

January 2017

page 14/22

SPIFAN II SLV kit product #3: Adult Nutritional RTF, High Protein (Placebo)

SPIFAN II SLV kit product #4: Adult Nutritional RTF, High Fat (Placebo)

1.308

2.127

2.482

AMQ - 2.803

NH3 - 3.283

His - 3.655

mono-LYS - 4.556

Ser - 6.126

Arg - 7.054

Gly - 7.523

7.970

Asp - 9.237

9.746

9.951

10.782

11.147

11.284

11.508

Glu - 12.020

12.864

13.174

Thr - 13.532

13.937

14.290

Ala - 14.580

14.815

15.048 15.078 15.135 15.202 15.258

15.572

Pro - 15.727

15.841 15.899 15.951

16.140 16.226 16.272 16.338

16.495

16.637 16.741 16.827

Deriv Peak - 16.955

17.069 17.146

Lys - 17.261

Tyr - 17.630

xCys - 17.914 Met - 18.018

Val - 18.289

NVa - 18.594

18.669

18.875 18.979

19.128

19.365 19.418

19.713

19.843

Ile - 20.074

Leu - 20.293

20.484

Phe - 20.584

20.929

21.184

21.582 21.629 21.688 21.754 21.794 21.847

21.966

AU

0.00

0.02

0.04

0.06

0.08

0.10

0.12

0.14

0.16

0.18

0.20

0.22

0.24

0.26

0.28

0.30

0.32

0.34

0.36

0.38

0.40

0.42

0.44

0.46

0.48

0.50

0.52

0.54

Minutes

1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00

2.208

2.567

AMQ - 2.970

NH3 - 3.544

His - 4.057

mono-LYS - 5.084

6.586

Ser - 6.819

Arg - 8.051

Gly - 8.352

8.835

Asp - 10.250

10.680

11.264

Glu - 12.670

13.260

Thr - 13.899

Ala - 14.845

Pro - 15.909

16.942

Deriv Peak - 17.072

Lys - 17.369

17.483

Tyr - 17.773

xCys - 18.047 Met - 18.150

Val - 18.402

NVa - 18.703

18.981

19.492

Ile - 20.163

Leu - 20.379

Phe - 20.688

20.991

21.765 21.874

AU

0.000

0.010

0.020

0.030

0.040

0.050

0.060

0.070

0.080

0.090

0.100

0.110

0.120

0.130

0.140

0.150

0.160

0.170

0.180

0.190

0.200

0.210

0.220

0.230

0.240

0.250

Minutes

1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00

AMINO-01 (FEBRUARY 2017) - APPENDICES

FOR ERP USE ONLY

DO NOT DISTRIBUTE