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Silliker
Chem, Res. Center Crete, IL – Validation of a LC-MS/MS Method for Vitamin K Analysis
Silliker Laboratories, Chemistry Research Center, Date: 1/30/15
18
Sample #6
Stdev
0.4
0.0
0.4
% RSD
4.5
0.0
4.0
n
2
2
2
SPIFAN
Sample #7
Mean
1.7
1.0
2.7
Stdev
0.0
0.0
0.0
% RSD
1.5
3.0
1.8
n
2
2
2
SPIFAN
Sample #8
Mean
5.9
1.0
6.9
Stdev
0.9
0.2
1.1
% RSD
15.8
15.3
15.7
n
2
2
2
SPIFAN
Sample #9
Mean
6.6
1.0
7.5
Stdev
0.3
0.1
0.5
% RSD
4.8
12.5
6.4
n
3
3
3
SPIFAN
Sample #10
Mean
2.3
0.3
2.6
Stdev
0.0
0.0
0.1
% RSD
2.2
3.7
2.4
n
3
3
3
SPIFAN
Sample #11
Mean
2.2
0.4
2.6
Stdev
0.2
0.0
0.2
% RSD
8.5
5.8
8.1
n
3
3
3
SPIFAN
Sample #12
Mean
6.9
0.9
7.8
Stdev
0.2
0.0
0.2
% RSD
2.8
5.5
2.8
n
3
3
3
SPIFAN
Sample #13
Mean
4.6
1.0
5.6
Stdev
0.2
0.0
0.2
% RSD
4.5
4.3
4.4
n
3
3
3
SPIFAN
Sample #14
Mean
5.4
1.1
6.5
Stdev
0.3
0.1
0.3
% RSD
4.8
5.2
4.9
n
3
3
3
SPIFAN
Sample #15
Mean
7.6
1.5
9.0
Stdev
0.1
0.0
0.1
% RSD
1.8
2.7
1.1
n
3
3
3
SPIFAN
Sample #16
Mean
6.4
2.0
8.4
Stdev
0.5
0.1
0.6
% RSD
7.7
7.2
7.6
n
3
3
3
SPIFAN
Sample #17
Mean
7.9
2.8
10.7
Stdev
0.6
0.1
0.7
% RSD
7.4
2.6
6.2
n
3
3
3
VitK-01 w/SLV
FOR ERP USE ONLY
DO NOT DISTRIBUTE