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Natural Remedies Pvt Ltd.

Quality control Dept.

Sample ID : 12-Deoxy withastramonolide

Method Name

: C:\CLASS-VP\Methods\METHODS\Withania.met

Data Name

: D:\2007\Method validation\Withania somnifera\Jan 2007\160107\spl-04a

Injection Volume

: 20

Acquired

: 1/16/07 8:23:39 PM

Minutes

0

5

10

15

20

25

30

35

40

45

mAU

0

250

500

750

1000

1250

mAU

0

250

500

750

1000

1250

21.397

22.368

23.211

Detector

A-227 nm

Retention

Time

Area Area

Percent

Resolution Asymmetry Theoretica

l plates

Capacity

factor

Width USP

Width

Height

21.397

47071

0.70

0.00

1.14

218371.22 0.24

0.41 0.18 6927

22.368 6561291 97.03

5.56

1.03

290232.75 0.30

0.43 0.17 108561

1

23.211

153754 2.27

5.02

1.14

298543.09 0.35

0.42 0.17 25530

Totals

6762116 100.00

111806

8

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