210 / 227
1$785$/ 5(0(',(6
3DJH RI
Table-58:
RD/1162-RM
: Weight of sample: 755.9
mg
- 100ml with methanol
Marker
Actual
content
(% w/w)
Weight
of
sample
(mg)
Actual
quantity
in the
weight
taken
Quantity
added
(mg)
Purity
Total
Quantity
(mg)
Calculated
Values
(%w/w)
Observed
Value
(%w/w)
Recovery
(%w/w)
W-IV
0.121
0.915
0.96
90
1.779
0.233
0.230
99.01
W-V
0.094
0.711
2.43
90
1.585
0.207
0.198
95.34
WF-A
0.089
0.673
1.26
99
1.920
0.251
0.248
98.79
12-D
0.018
0.136
1.22
95
1.295
0.169
0.155
91.18
W –A
0.023
0.174
1.25
99
1.411
0.185
0.174
94.47
W –B
0.006
755.9
0.045
1.07
99
1.105
0.145
0.141
97.51
Table-59: WS/06LOT08: Weight of sample: 1714.4
mg
- 100ml with methanol
Actual quantity in
the weight taken
Marker
Actual
content
(% w/w)
Weight
of
sample
(mg)
100 ml
1 ml
Quanti
ty
added
(mg)
Purity
Total
Quantity
(mg)
Calculated
Values
(%w/w)
Observed
Value
(%w/w)
Recovery
(%w/w)
W-IV
0.798
13.7
0.137
0.164
90
0.284
1.571
1.580
100.58
W-V
0.700
12.0
0.120
0.056
90
0.170
0.941
0.940
99.84
WF-A
0.644
11.0
0.110
0.230
99
0.338
1.868
1.865
99.86
12-D
0.278
4.8
0.048
0.190
95
0.228
1.261
1.271
100.86
W –A
0.226
3.9
0.039
0.160
99
0.197
1.089
1.059
97.26
W –B
0.067
1714.4
1.1
0.011
0.156
99
0.166
0.917
0.688
75.03
Table-601: WS/05LOT20: Weight of sample: 5029.7mg - 100ml with methanol
Actual quantity in
the weight taken
Marker
Actual
content
(% w/w)
Weight
of
sample
(mg)
100 ml
1 ml
Quanti
ty
added
(mg)
Purity
Total
Quantity
(mg)
Calculated
Values
(%w/w)
Observed
Value
(%w/w)
Recovery
(%w/w)
W-IV
0.053
2.7
0.027
0.164
90
0.174
0.340
0.345
101.50
W-V
0.044
2.2
0.022
0.056
90
0.073
0.142
0.142
100.06
WF-A
0.069
3.5
0.035
0.230
99
0.262
0.512
0.510
99.55
12-D
0.019
1.0
0.010
0.190
95
0.190
0.371
0.375
101.02
W –A
0.020
1.0
0.010
0.160
99
0.168
0.329
0.323
98.41
W –B
0.005
5029.7
0.3
0.003
0.156
99
0.157
0.306
0.226
73.69
Table-61: RD/1045: Weight of sample: 1640.2mg - 100ml with methanol
Actual quantity in
the weight taken
Marker
Actual
content
(% w/w)
Weight
of
sample
(mg)
100 ml
1 ml
Quanti
ty
added
(mg)
Purity
Total
Quantity
(mg)
Calculated
Values
(%w/w)
Observed
Value
(%w/w)
Recovery
(%w/w)
W-IV
0.552
9.1
0.091
0.164
90
0.238
1.372
1.369
99.81
W-V
0.416
6.8
0.068
0.056
90
0.119
0.683
0.685
100.28
WF-A
0.408
6.7
0.067
0.230
99
0.295
1.697
1.702
100.27
12-D
0.253
4.1
0.041
0.190
95
0.222
1.279
1.296
101.35
W –A
0.137
2.2
0.022
0.160
99
0.181
1.042
1.003
96.29
W –B
0.045
1640.2
0.7
0.007
0.156
99
0.162
0.932
0.698
74.88