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Table 2014.2A

: Comparative Results for the Detection of

Listeriamonocytogenes

in Full Fat Cottage Cheese (4% Milk Fat) by the 3M

MDA

1

Listeriamonocytogenes

Method vs. AOAC OMA 993.12 in a Collaborative Study (Uninoculated Control)

2

Statistic

MPN/

Test

Portion

Laboratory

Candidate presumptive

(CP)

Candidate confirmed (CC)

Candidate result (C)

Reference method (R)

C vs. R

N

X

POD

(CP)

N

X

POD

(CC)

N

X

POD

(C)

N

X

POD

(R)

dLPOD

(C,R)

dLPOD

(CP,CC)

1

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

2

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

3

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

4

a

NA

f

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

5

a

NA NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

6

a

12

1

0.08

12

12

1.00

12

1

0.08

12

0

0.00

0.08

1.00

7

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

8

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

9

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

10

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

11

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

12

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

13

a

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

14

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

15

12

0

0.00

12

0

0.00

12

0

0.00

12

0

0.00

0.00

0.00

Estimate

All

132

0

0.00

132

0

0.00

132

0

0.00

132

0

0.00

0.00

0.00

LCL

0.00

0.00

0.00

0.00

-0.03

-0.03

UCL

0.03

0.03

0.03

0.03

0.03

0.03

s

r

b

0.00

0.00

0.00

0.00

LCL

0.00

0.00

0.00

0.00

UCL

0.16

0.16

0.16

0.16

s

L

c

0.00

0.00

0.00

0.00

LCL

0.00

0.00

0.00

0.00

UCL

0.16

0.16

0.16

0.16

s

R

d

0.00

0.00

0.00

0.00

UCL

0.00

0.00

0.00

0.00

LCL

0.23

0.23

0.23

0.23

P

T

e

1.0000

1.0000

1.0000

1.0000

a

Results were not used in statistical analysis due to deviation from testing protocol.

3

b

Repeatability Standard Deviation,

c

Among-Laboratory Standard Deviation,

d

Reproducibility Standard Deviation,

e

P

T

Value =Homogeneity test of laboratory PODs,

f

NA- laboratory results were not received

4

LCL – Lower Confidence Limit; UCL – Upper Confidence Limit

5

Candidates for 2016 Method of the Year

171