AOAC SPIFAN ERP Meeting Book (3-16-16)

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Validation Parameter
Test Group Name Date 01.01.2015
Test Name Data Path File 2015\January\Vitamins\01.01.2015
Matrix Raw-Data File Ref. TUV/BLR/F-360
Equiment Analyst Manjunath K/Prasad BKVR
With Multilevel Calibration
Calibration Standards Concentration (ug/kg) Area-Analyte
Solvent Standard Level-1 5.00 2477.66
Solvent Standard Level-2 10.00 4656.99
Solvent Standard Level-3 50.00 22902.51
Solvent Standard Level-4 100.00 41547.43
Solvent Standard Level-5 200.00 77155.21
Solvent Standard Level-6 300.00 113644.70
Criteria R2 ≥ 0.99
Conclusion Complies
Page 16
LC-MS/MS 6460A (BLR/PS-CRS/006.03)
AOAC- SPIFAN-2012-VITAMINS
Calibration Curve
B-complex Vitamins
Nicotinic acid
Aqueous
y = 374.38x + 2237.4
R² = 0.9987
0.00
20000.00
40000.00
60000.00
80000.00
100000.00
120000.00
140000.00
0.00 50.00 100.00 150.00 200.00 250.00 300.00 350.00
BVit-03 (February 2016)
FOR ERP USE ONLY
DO NOT DISTRIBUTE