AOAC SPIFAN ERP Meeting Book (3-16-16)

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Validation Parameter
Test Group Name Date 01.01.2015
Test Name Data Path File 2015\January\Vitamins\01.01.2015
Matrix Raw-Data File Ref. TUV/BLR/F-360
Equiment Analyst Manjunath K/Prasad BKVR
With Multilevel Calibration
Calibration Standards Concentration (ug/kg) Area-Analyte
Solvent Standard Level-1 5.00 6997.95
Solvent Standard Level-2 20.00 29377.70
Solvent Standard Level-3 50.00 75320.57
Solvent Standard Level-4 100.00 150423.73
Solvent Standard Level-5 400.00 545240.86
Solvent Standard Level-6 500.00 621801.71
Criteria R2 ≥ 0.99
Conclusion Complies
Page 17
LC-MS/MS 6460A (BLR/PS-CRS/006.03)
AOAC- SPIFAN-2012-VITAMINS
Calibration Curve
B-complex Vitamins
Pantothenic acid
Aqueous
y = 1269.4x + 10759
R² = 0.9957
0.00
100000.00
200000.00
300000.00
400000.00
500000.00
600000.00
700000.00
0.00 100.00 200.00 300.00 400.00 500.00 600.00
BVit-03 (February 2016)
FOR ERP USE ONLY
DO NOT DISTRIBUTE