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Method Performance Feedback 2012.01

AOAC OMA 2014.08

POLYCYLIC AROMATIC HYDROCARBONS IN SEAFOOD GAS CHROMOTOGRAPHY MASS SPECTROMETRY

Was the method's applicability considered?

Please state the method's applicability statement:

Yes

Applicable for the determination of 32 PAH's in mussel, oyster, and shrimp.

Yes

Applicable for the determination of the following PAHs in mussel, oyster, and shrimp: 1,7-

dimethylphenanthrene, 1-methylnaphthalene, 1-methylphenanthrene, 2,6-dimethylnaphthalene,

3-methylchrysene, anthracene, benz[a]anthracene, benzo[a]pyrene, benzo[b]fluoranthene,

benzo[g, b,h,i]perylene, benzo[k] fluoranthene, chrysene, dibenz[a,h]anthracene, fluoranthene,

fluorine, indeno[1,2,3-cd]pyrene, naphthalene, phenanthrene, and pyrene. These were

representative PAH analytes selected for the collaborative study. The method has been single

laboratory validated for 32 PAHs in fish and shrimp and therefore, is expected to be applicable to

other GC-amenable PAHs and seafood matrices.

Yes

This method was developed in response to the most recent oil spill in the Gulf coast.

Yes

Applicable for the determination of the following PAHs

in mussel, oyster, and shrimp: 1,7-dimethylphenanthrene,

1-methylnaphthalene, 1-methylphenanthrene, 2,6-dimethylnaphthalene,

3-methylchrysene, anthracene, benz[a]anthracene,

benzo[a]pyrene, benzo[b]fluoranthene, benzo[g,h,i]perylene,

benzo[k]fluoranthene, chrysene, dibenz[a,h]anthracene,

fluoranthene, fluorene, indeno[1,2,3-cd]pyrene, naphthalene,

phenanthrene, and pyrene. These were representative PAH analytes

selected for the collaborative study. The method has been singlelaboratory

validated for 32 PAHs in fish and shrimp (1), and,

therefore, is expected to be applicable to other GC-amenable PAHs

and seafood matrices. The concentration ranges evaluated within

the collaborative study are given in Table 2014.08A.]

Yes

Applicable for the determination of the following PAHs in mussel, oyster, and shrimp: 1,7-

dimethylphenanthrene, 1-methylnaphthalene, 1-methylphenanthrene, 2,6-dimethylnaphthalene,

3-methylchrysene, anthracene, benz[a]anthracene, benzo[a]pyrene, benzo[b]fluoranthene,

benzo[g,h,i]perylene, benzo[k]fluoranthene, chrysene, dibenz[a,h]anthracene, fluoranthene,

fluorine, indeno[1,2,3-cd]pyrene, naphthalene, phenanthrene, and pyrene. These were

representative PAH analytes selected for the collaborative study. The method has been single-

laboratory validated for 32 PAHs in fish and shrimp, and, therefore, is expected to be applicable to

other GC-amenable PAHs and seafood matrices.

Yes

[Applicable for the determination of the following PAHs in mussel, oyster and shrimp: 1,7-

dimethylphenanthene, 1-methylnaphthalene, 1-methylphenanthrene, 2,6-dimethylnaphthalene,

3-methylchrysene, anthracene, benz[a]anthracene, benzo[a]pyrene, benzo[b]fluoranthene,

benzo[g,h,i]perylene, [k]fluoranthene, chrysene, dibenz[a,h]anthraccene, fluoranthene, Fluorene,

indeno[1,2,3-cd]pyrene, naphthalene, phenanthrene, and pyrene. These were representative PAH

analytes selected for the collaborative study. The method has been single-laboratory validated for

32 PAHs in fish and shrimp and, therefore, is expected to be applicable to other GC-amenable PAHs

and seafood matrices.]