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Validation data – method performance characteristics
Smoked salmon
– spiked concentrations – 1 and 5 μg/kg
Concentration level 1 μg/kg
Analyte
Spike 1 Spike 2
Spike 3
Spike 4
Spike 5
Spike 6
Recovery
(%)
Repeatab
ility, RSD
(%)
LOQ (μg/kg)
Linearity range
(μg/kg)
BcFln
106
103
108
107
98
99
104
4
0.05
0.05 - 100
BaA
103
97
100
97
94
94
97
4
0.03
0.03 - 100
CPcdP
82
82
82
90
91
91
86
5
0.03
0.03 - 100
Chr
109
101
106
101
101
107
104
3
0.03
0.03 - 100
5 MeCHr
85
88
86
86
83
87
86
2
0.05
0.03 - 100
BbF
84
82
88
86
88
87
86
3
0.03
0.03 - 100
BkF
94
98
102
98
97
91
97
5
0.03
0.03 - 100
BjF
100
101
101
94
93
93
97
4
0.03
0.03 - 100
BaP
93
90
95
96
91
90
93
3
0.03
0.03 - 100
IcdP
94
100
93
70
83
84
91
4
0.03
0.03 - 100
DbahA
86
83
81
83
80
82
83
3
0.03
0.03 - 100
BghiP
100
102
101
101
102
103
101
1
0.03
0.03 - 100
DBalP
98
91
97
93
88
93
93
4
0.10
0.10 - 100
DBaeP
91
95
92
97
90
91
93
3
0.10
0.10 - 100
DBaiP
95
98
98
99
95
93
98
2
0.10
0.10 - 100
DBahP
79
60
95
82
82
93
88
8
0.10
0.10 - 100