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4
Concentration level 5 μg/kg
Analyte
Spike 1 Spike 2
Spike 3
Spike 4
Spike 5
Spike 6
Recovery
(%)
Repeatabili
ty, RSD (%)
LOQ (μg/kg)
Linearity range
(μg/kg)
Naph
70
80
55
70
80
84
77
8
0.10
0.10 - 100
Ace
84
89
78
86
90
90
86
6
0.10
0.10 - 100
Fln
77
83
75
80
85
84
81
5
0.05
0.05 - 100
Phe
80
85
81
84
90
86
84
4
0.05
0.05 - 100
Ant
77
81
79
79
78
79
79
2
0.05
0.05 - 100
Flt
108
115
51
99
102
116
108
7
0.05
0.05 - 100
Pyr
76
83
84
85
85
82
82
4
0.05
0.05 - 100
BaA
85
89
86
87
93
89
88
3
0.05
0.05 - 100
Chr
86
90
86
89
93
90
89
3
0.05
0.05 - 100
BbF
84
90
89
93
93
89
90
4
0.05
0.05 - 100
BkF
89
93
91
94
96
92
93
3
0.05
0.05 - 100
BaP
87
92
90
93
96
92
92
3
0.05
0.05 - 100
DBahA
88
93
90
93
94
92
92
3
0.05
0.05 - 100
BghiP
89
95
92
96
98
93
94
3
0.05
0.05 - 100
IcdP
91
96
93
98
100
95
95
4
0.05
0.05 - 100