AOAC-RI ERP Book - FAOM METHOD.pdf

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M ASTOVSKA ET AL.: JOURNAL OF AOAC INTERNATIONAL VOL. 98, N O. 2, 2015 479
Collaborative Study
Purpose
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intralaboratory and interlaboratory performance and submit the
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Method for the determination of PAHs in seafood.
Study Design
This study evaluated the method performance for
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relevant to an oil spill contamination (see Table 1), in three
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were followed for the preparation of the study and data analysis.
Test Sample Preparation
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a blank. Participants were supplied with the test samples ready
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themselves on the day of the analysis.
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of the shrimp test sample preparation protocol (as compared to
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preparation and shipment of the new set of shrimp samples to
the study participants.)
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and evaporation techniques and equipment. Therefore,
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phase, but only 10 of them (listed in the Acknowledgments
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continued in the study.
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participants prepared calibration standards and obtained
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concentration levels, a limited calibration curve (without
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