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Validation data – method performance characteristics
Shrimps
– spiked concentrations – 1 and 5 μg/kg
Concentration level 1 μg/kg
Analyte
Spike 1 Spike 2
Spike 3
Spike 4
Spike 5
Spike 6
Recovery
(%)
Repeatabili
ty, RSD (%)
LOQ (μg/kg)
Linearity range
(μg/kg)
Naph
77
80
81
77
86
67
78
9
0.1
0.10 - 100
Ace
72
79
82
84
75
84
79
6
0.1
0.10 - 100
Fln
80
79
80
93
79
87
83
7
0.05
0.05 - 100
Phe
80
72
87
86
68
80
79
9
0.05
0.05 - 100
Ant
75
73
76
85
74
85
78
7
0.05
0.05 - 100
Flt
100
87
101
97
96
103
97
6
0.05
0.05 - 100
Pyr
89
78
82
93
80
89
85
7
0.05
0.05 - 100
BaA
82
88
83
92
82
89
86
5
0.05
0.05 - 100
Chr
84
79
84
96
83
91
86
7
0.05
0.05 - 100
BbF
84
82
87
98
81
93
88
8
0.05
0.05 - 100
BkF
87
84
90
100
85
97
91
7
0.05
0.05 - 100
BaP
87
84
89
99
84
95
90
7
0.05
0.05 - 100
DBahA
89
85
91
100
87
97
91
6
0.05
0.05 - 100
BghiP
88
85
91
99
87
97
91
6
0.05
0.05 - 100
IcdP
89
86
92
100
86
100
92
7
0.05
0.05 - 100