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M
ASTOVSKA
ET AL
.
J
OURNAL OF
AOAC I
NTERNATIONAL
V
OL
. 98, N
O
. 2, 2015
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preparation and extraction) in comparison with currently
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complete. In addition, acceptable methods had to demonstrate
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of reference materials), and practical considerations, such as
availability of equipment.
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method was studied within the presented collaborative study, for
which the analytes were narrowed down to include only PAHs
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see
Table 1 for the
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Table 1. PAHs included in the collaborative study
Name
Abbreviation
1,7-Dimethylphenanthrene
1,7-DMP
1-Methylnaphthalene
1-MN
1-Methylphenanthrene
1-MP
2,6-Dimethylnaphthalene
2,6-DMN
3-Methylchrysene
3-MC
Anthracene
Ant
Benz[
a
]anthracene
BaA
Benzo[
a
] pyrene
BaP
Benzo[
b
@ÀXRUDQWKHQH
BbF
Benzo[
g,h,i
]perylene
BghiP
Benzo[
k
@ÀXRUDQWKHQH
BkF
Chrysene
Chr
Dibenz[
a,h
]anthracene
DBahA
)OXRUDQWKHQH
Flt
)OXRUHQH
Fln
Indeno[1,2,3-
cd
]pyrene
IcdP
Naphthalene
Naph
Phenanthrene
Phe
Pyrene
Pyr
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Shrimp
0XVVHO
Oyster
Low
Mid
High
Low
Mid
High
Low
Mid
High
PAH
Level 1
Level 2
Level 4
Level 1
Level 3
Level 4
Level 2
Level 3
Level 5
1,7-DMP
a
20
20
20
40
40
40
80
80
80
1-MN
20
75
200
20
100
200
75
100
250
1-MP
10
25
125
10
50
125
25
50
200
2,6-DMN
15
40
175
15
75
175
40
75
225
3-MC
10
30
145
10
90
145
30
90
225
Ant
5
10
40
5
15
40
10
15
60
BaA
5
15
60
5
25
60
15
25
100
BaP
2
5
25
2
10
25
5
10
50
BbF
5
10
75
5
30
75
10
30
100
BghiP
2
5
20
2
10
20
5
10
25
BkF
2
8
40
2
20
40
8
20
75
Chr
15
50
175
15
100
175
50
100
250
DBahA
2
5
15
2
10
15
5
10
20
Fln
5
15
50
5
25
50
15
25
75
Flt
10
25
100
10
50
100
25
50
150
IcdP
2
5
20
2
10
20
5
10
25
Naph
25
80
160
25
125
160
80
125
225
Phe
15
50
175
15
100
175
50
100
250
Pyr
15
40
125
15
75
125
40
75
200
a
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