ASH-001_AOAC_Withania_Submission

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Table-43: B. No. WS/06Lot08
Replicate Withanoside
IV
Withanoside
V
Withaferin
A
12-Deoxy
withastramonolide
Withanolide A Withanolide
B
Sum
Replicate - 1 0.908 0.638 0.652 0.281 0.223 0.066 2.768
Replicate - 2 0.921 0.654 0.663 0.286 0.227 0.067 2.818
Replicate - 3 0.921 0.658 0.662 0.285 0.226 0.066 2.819
Mean 0.917 0.650 0.659 0.284 0.225 0.066 2.802
RSD 0.85 1.61 0.89 0.93 0.86 0.71 1.03
Table-44: B.
Replicate Withanoside
IV
Withanoside
V
Withaferin
A
12-Deoxy
withastramonolide
Withanolide A Withanolide
B
Sum
Replicate - 1 0.909 0.615 0.615 0.267 0.205 0.063 2.673
Replicate - 2 0.912 0.627 0.616 0.267 0.205 0.062 2.690
Replicate - 3 0.911 0.621 0.615 0.266 0.206 0.062 2.682
Mean 0.911 0.621 0.616 0.267 0.205 0.062 2.681
RSD 0.21 0.97 0.09 0.20 0.29 0.31 0.32
Table-45: B.
Replicate Withanoside
IV
Withanoside
V
Withaferin
A
12-Deoxy
withastramonolide
Withanolide A Withanolide
B
Sum
Replicate - 1 0.070 0.046 0.085 0.024 0.022 0.006 0.253
Replicate - 2 0.067 0.044 0.080 0.022 0.021 0.005 0.239
Replicate - 3 0.064 0.042 0.077 0.021 0.020 0.005 0.231
Mean 0.067 0.044 0.081 0.022 0.021 0.005 0.241
RSD 4.50 3.92 4.68 5.13 5.46 3.68 4.56
Table-46: B.
Replicate Withanoside
IV
Withanoside
V
Withaferin
A
12-Deoxy
withastramonolide
Withanolide A Withanolide
B
Sum
Replicate - 1 0.477 0.307 0.410 0.125 0.102 0.029 1.450
Replicate - 2 0.478 0.311 0.410 0.125 0.102 0.029 1.455
Replicate - 3 0.479 0.311 0.411 0.124 0.102 0.029 1.456
Mean 0.478 0.310 0.410 0.125 0.102 0.029 1.453
RSD 0.22 0.71 0.15 0.46 0.21 0.49 0.23
Table-47: B.
Replicate Withanoside
IV
Withanoside
V
Withaferin
A
12-Deoxy
withastramonolide
Withanolide A Withanolide
B
Sum
Replicate - 1 0.861 0.605 0.708 0.337 0.233 0.077 2.821
Replicate - 2 0.844 0.588 0.697 0.330 0.227 0.076 2.762
Replicate - 3 0.839 0.588 0.695 0.330 0.227 0.076 2.755
Mean 0.848 0.594 0.700 0.332 0.229 0.076 2.779
RSD 1.37 1.65 1.04 1.16 1.54 0.97 1.32