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Parameter
Acceptance Criteria
R2
≥ 0.99
For ≤ 10 μg/l : 70-125 %
10-1000 μg/l : 75-120 %
Accuracy
70 - 125 %
Precision (RSD %)
≤ 15 %
Least/Most intesne
ion ratio
Maximum tolerance (relative)
0.50 - 1.00
± 30 %
0.20 - 0.50
± 30 %
0.10 - 0.20
± 30 %
<0.10
± 30 %
RT ratio
0.95 - 1.05
Concentration
Recovery limits, %
≤ 10 μg/kg
70 - 125
1.0 mg/kg
75 - 120
10 mg/kg
80 - 115
0.01 g/100g
85 - 110
0.1 g/100g
90 - 108
1.0 g/100g
92 - 105
10 g/100g
95 - 102
100 g/100g
98 - 101
Concentration
Repeatability (RSDr), %
≤ 10 μg/kg
15
1.0 mg/kg
8
10 mg/kg
6
0.01 g/100g
4
0.1 g/100g
3
1.0 g/100g
2
10 g/100g
1.5
100 g/100g
1
Concentration
Repeatability (RSD
R
), %
≤ 10 μg/kg
32
1.0 mg/kg
16
10 mg/kg
11
0.01 g/100g
8
0.1 g/100g
3
1.0 g/100g
2
10 g/100g
1.5
100 g/100g
1
Page 4
Accuracy
Table : Validation parameters and Acceptance Criteria for B- Vitamins
Validation Parameter
Criteria
Repeatability Precision (RSDr)
Reproducibility Precision (RSD
R
)
Linearity/Calibration fit
Back calculated
values accuracy
LOQ
Specificity
Ion Ratio
BVit-03 (February 2016)
FOR ERP USE ONLY
DO NOT DISTRIBUTE