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Dual Lab Validation of a Method for the Determination of Fructans in Infant
Formula & Adult Nutritionals /
25 Jul 2016
58
Results calibration test 21 June 2016
Fructose calibration ISC 3000_D instrument
Fructose
range: 0.894 – 178.7 mg/l
y = 0.811 x
2
+ 18.129 x + 0.251 R
2
= 0.9998
Glucose calibration ISC 3000_D instrument
Glucose
range 0.051 – 20.49
mg/l y = 0.044 x
2
+ 5.754 x +0.003 R
2
= 1.000
respons
glucose
glucose
Glucose/chitobise
conc
calculated
lack of fit
mg/l
mg/l
absolute %
0,0093
0,0512
0,05622
‐0,0050
‐9,7
0,0182
0,1025
0,10763
‐0,0052
‐5,0
0,0350
0,2049
0,20406
0,0009
0,4
0,0519
0,3074
0,30118
0,0062
2,0
0,0881
0,5123
0,51022
0,0021
0,4
0,171
1,025
0,989
0,035
3,5
0,354
2,049
2,043
0,006
0,3
0,615
3,586
3,560
0,026
0,7
0,900
5,123
5,220
‐0,097
‐1,9
1,761
10,25
10,27
‐0,03
‐0,3
2,601
15,37
15,27
0,10
0,7
3,475
20,49
20,54
‐0,04
‐0,2
respons
fructose fructose
Fructose/chitobiose
conc
calculated
lack of fit
mg/l
mg/l
abs
%
0,050
0,894
0,954
‐0,060
‐6,7
0,075
1,341
1,387
‐0,046
‐3,5
0,126
2,234
2,277
‐0,043
‐1,9
0,253
4,469
4,525
‐0,056
‐1,3
0,501
8,937
8,951
‐0,014
‐0,2
0,886
15,64
15,93
‐0,29
‐1,9
1,22
22,34
22,16
0,18
0,8
2,47
44,69
45,90
‐1,22
‐2,7
3,49
67,03
66,22
0,81
1,2
4,74
89,37
92,43
‐3,06
‐3,4
6,47
134,1
130,5
3,5
2,6
8,56
178,7
180,1
‐1,4
‐0,8
VALIDATION REPORT
FOR ERP USE ONLY
DO NOT DISTRIBUTE