AOAC SPIFAN Review Team (August 2016)

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Dual Lab Validation of a Method for the Determination of Fructans in Infant
Formula & Adult Nutritionals /
25 Jul 2016
59
ANNEX C Experimental data LOD and LOQ
Experimental data of the LOD and LOQ determination in the fructan spiked reconstituted sample no 7,
Infant formula powder partially hydrolyzed milk based.
repetition
no
date
28 Februari 2016 23 May 2016
Fructan concentration (%) Fructan concentration (%)
1 0,044 0,047
2 0,044 0,044
3 0,043 0,045
4 0,042 0,046
5 0,042 0,045
6 0,045 0,051
7 0,044 0,049
8 0,047 0,050
9 0,045 0,049
10 0,046 0,053
average 0,044 0,048
SDr 0,002 0,003
LOD 0,005 0,009
LOQ 0,016 0,030
VALIDATION REPORT
FOR ERP USE ONLY
DO NOT DISTRIBUTE