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Single Lab Validation of a Method for the Determination of β‐
Galactooligosaccharides in Infant Formula & Adult Nutritionals / Sean Austin (NRC,
Lausanne)
25 Jul 2016
CONFIDENTIAL
∙ This document may not be reproduced or disclosed to third parties without prior authorization
Page 28 / 35
3.
RAW DATA (TRUENESS)
Spike‐Recovery: Sample KBI‐00045
Date
Analyst Instrument Sample GOS
GOS
Spike
Level
(g/100g)
Measured
GOS
(g/100g)
Recovery
(%)
Average
(%)
RSD
(%)
02.06.2016
CMu
RS #2 KBI‐00045 Vivinal
0.211
0.177
83.9
02.06.2016
CMu
RS #2 KBI‐00045 Vivinal
0.211
0.178
84.4
10.06.2016
dc
RS #3 KBI‐00045 Vivinal
0.211
0.188
89.1
10.06.2016
dc
RS #3 KBI‐00045 Vivinal
0.211
0.19
90.0
09.06.2016
CMu
RS #2 KBI‐00045 Vivinal
0.211
0.168
79.6
09.06.2016
CMu
RS #2 KBI‐00045 Vivinal
0.211
0.172
81.5
02.06.2016
CMu
RS #2 KBI‐00045 Clasado 0.980
0.857
87.4
02.06.2016
CMu
RS #2 KBI‐00045 Clasado 0.980
0.856
87.3
10.06.2016
dc
RS #3 KBI‐00045 Clasado 0.980
0.873
89.1
10.06.2016
dc
RS #3 KBI‐00045 Clasado 0.980
0.872
89.0
09.06.2016
CMu
RS #2 KBI‐00045 Clasado 0.980
0.822
83.9
09.06.2016
CMu
RS #2 KBI‐00045 Clasado 0.980
0.827
84.4
02.06.2016
CMu
RS #2 KBI‐00045 Vivinal
2.47
2.24
90.7
02.06.2016
CMu
RS #2 KBI‐00045 Vivinal
2.47
2.23
90.3
10.06.2016
dc
RS #3 KBI‐00045 Vivinal
2.47
2.18
88.3
10.06.2016
dc
RS #3 KBI‐00045 Vivinal
2.47
2.18
88.3
17.06.2016
dc
RS #3 KBI‐00045 Vivinal
2.47
2.16
87.4
17.06.2016
dc
RS #3 KBI‐00045 Vivinal
2.47
2.24
90.7
02.06.2016
CMu
RS #2 KBI‐00045 Clasado 4.91
4.26
86.8
02.06.2016
CMu
RS #2 KBI‐00045 Clasado 4.91
4.27
87.0
10.06.2016
dc
RS #3 KBI‐00045 Clasado 4.91
4.29
87.4
10.06.2016
dc
RS #3 KBI‐00045 Clasado 4.91
4.31
87.8
09.06.2016
CMu
RS #2 KBI‐00045 Clasado 4.91
4.04
82.3
09.06.2016
CMu
RS #2 KBI‐00045 Clasado 4.91
4.06
82.7
Recovery
84.8
4.9
85.6
2.9
86.9
2.6
89.3
1.6
VALIDATION REPORT
FOR ERP USE ONLY
DO NOT DISTRIBUTE