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Single Lab Validation of a Method for the Determination of β‐
Galactooligosaccharides in Infant Formula & Adult Nutritionals / Sean Austin (NRC,
Lausanne)
25 Jul 2016
CONFIDENTIAL
∙ This document may not be reproduced or disclosed to third parties without prior authorization
Page 29 / 35
Spike‐Recovery: Sample KBI‐00046
Date
Analyst Instrument Sample GOS
GOS
Spike
Level
(g/100g)
Measured
GOS
(g/100g)
Recovery
(%)
Average
(%)
RSD
(%)
02.06.2016
CMu
RS #2 KBI‐00046 Vivinal
0.211 0.175
82.9
02.06.2016
CMu
RS #2 KBI‐00046 Vivinal
0.211 0.166
78.7
10.06.2016
dc
RS #3 KBI‐00046 Vivinal
0.211 0.191
90.5
10.06.2016
dc
RS #3 KBI‐00046 Vivinal
0.211 0.181
85.8
17.06.2016
dc
RS #3 KBI‐00046 Vivinal
0.211 0.225 106.6
17.06.2016
dc
RS #3 KBI‐00046 Vivinal
0.211 0.221 104.7
16.06.2016
CMu
RS #2 KBI‐00046 Clasado 0.990 0.858
86.7
16.06.2016
CMu
RS #2 KBI‐00046 Clasado 0.990 0.844
85.3
10.06.2016
dc
RS #3 KBI‐00046 Clasado 0.990 0.891
90.0
10.06.2016
dc
RS #3 KBI‐00046 Clasado 0.990 0.891
90.0
09.06.2016
CMu
RS #2 KBI‐00046 Clasado 0.990 0.961
97.1
09.06.2016
CMu
RS #2 KBI‐00046 Clasado 0.990
0.94
94.9
02.06.2016
CMu
RS #2 KBI‐00046 Vivinal
2.45
2.09
85.3
02.06.2016
CMu
RS #2 KBI‐00046 Vivinal
2.45
2.11
86.1
10.06.2016
dc
RS #3 KBI‐00046 Vivinal
2.45
2.18
89.0
10.06.2016
dc
RS #3 KBI‐00046 Vivinal
2.45
2.22
90.6
09.06.2016
CMu
RS #2 KBI‐00046 Vivinal
2.45
2.24
91.4
09.06.2016
CMu
RS #2 KBI‐00046 Vivinal
2.45
2.27
92.7
02.06.2016
CMu
RS #2 KBI‐00046 Clasado 4.97
4.35
87.5
02.06.2016
CMu
RS #2 KBI‐00046 Clasado 4.97
4.38
88.1
10.06.2016
dc
RS #3 KBI‐00046 Clasado 4.97
4.36
87.7
10.06.2016
dc
RS #3 KBI‐00046 Clasado 4.97
4.26
85.7
09.06.2016
CMu
RS #2 KBI‐00046 Clasado 4.97
4.24
85.3
09.06.2016
CMu
RS #2 KBI‐00046 Clasado 4.97
4.23
85.1
Recovery
91.5
12.7
86.6
1.6
90.7
5.1
89.2
3.3
VALIDATION REPORT
FOR ERP USE ONLY
DO NOT DISTRIBUTE