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Single Lab Validation of a Method for the Determination of β‐
Galactooligosaccharides in Infant Formula & Adult Nutritionals / Sean Austin (NRC,
Lausanne)
25 Jul 2016
CONFIDENTIAL
∙ This document may not be reproduced or disclosed to third parties without prior authorization
Page 31 / 35
Spike‐Recovery: Sample L3B‐00037
Date
Analyst Instrument Sample GOS
GOS
Spike
Level
(g/100g)
Measure
d GOS
(g/100g)
Recovery
(%)
Average
(%)
RSD
(%)
02.06.2016
dc
RS #3 L3B‐00037 Vivinal
0.202 0.229 113.4
02.06.2016
dc
RS #3 L3B‐00037 Vivinal
0.202 0.239 118.3
07.06.2016
dc
RS #3 L3B‐00037 Vivinal
0.202 0.234 115.8
07.06.2016
dc
RS #3 L3B‐00037 Vivinal
0.202 0.229 113.4
16.06.2016
CMu
RS #2 L3B‐00037 Vivinal
0.202 0.225 111.4
16.06.2016
CMu
RS #2 L3B‐00037 Vivinal
0.202 0.223 110.4
02.06.2016
dc
RS #3 L3B‐00037 Clasado 1.110 1.05
94.6
02.06.2016
dc
RS #3 L3B‐00037 Clasado 1.110 1.02
91.9
07.06.2016
dc
RS #3 L3B‐00037 Clasado 1.110 0.975 87.8
07.06.2016
dc
RS #3 L3B‐00037 Clasado 1.110 0.95
85.6
16.06.2016
CMu
RS #2 L3B‐00037 Clasado 1.110 0.961 86.6
16.06.2016
CMu
RS #2 L3B‐00037 Clasado 1.110 0.953 85.9
02.06.2016
dc
RS #3 L3B‐00037 Vivinal
2.36
2.28
96.6
02.06.2016
dc
RS #3 L3B‐00037 Vivinal
2.36
2.24
94.9
07.06.2016
dc
RS #3 L3B‐00037 Vivinal
2.36
2.24
94.9
07.06.2016
dc
RS #3 L3B‐00037 Vivinal
2.36
2.21
93.6
16.06.2016
CMu
RS #2 L3B‐00037 Vivinal
2.36
2.11
89.4
16.06.2016
CMu
RS #2 L3B‐00037 Vivinal
2.36
2.11
89.4
02.06.2016
dc
RS #3 L3B‐00037 Clasado 4.46
4.02
90.1
02.06.2016
dc
RS #3 L3B‐00037 Clasado 4.46
4.12
92.4
07.06.2016
dc
RS #3 L3B‐00037 Clasado 4.46
4.04
90.6
07.06.2016
dc
RS #3 L3B‐00037 Clasado 4.46
4.11
92.2
16.06.2016
CMu
RS #2 L3B‐00037 Clasado 4.46
3.82
85.7
16.06.2016
CMu
RS #2 L3B‐00037 Clasado 4.46
3.75
84.1
Recovery
113.8
2.6
89.2
3.9
88.7
4.2
93.1
3.3
VALIDATION REPORT
FOR ERP USE ONLY
DO NOT DISTRIBUTE