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Single Lab Validation of a Method for the Determination of β‐
Galactooligosaccharides in Infant Formula & Adult Nutritionals / Sean Austin (NRC,
Lausanne)
25 Jul 2016
CONFIDENTIAL
∙ This document may not be reproduced or disclosed to third parties without prior authorization
Page 30 / 35
Spike‐Recovery: Sample KBI‐00047
Date
Analyst Instrument Sample GOS
GOS
Spike
Level
(g/100g)
Measured
GOS
(g/100g)
Recovery
(%)
Average
(%)
RSD
(%)
02.06.2016
dc
RS #3 KBI‐00047 Vivinal
0.203 0.206 101.5
02.06.2016
dc
RS #3 KBI‐00047 Vivinal
0.203 0.212 104.4
07.06.2016
dc
RS #3 KBI‐00047 Vivinal
0.203 0.195
96.1
07.06.2016
dc
RS #3 KBI‐00047 Vivinal
0.203 0.201
99.0
16.06.2016
CMu
RS #2 KBI‐00047 Vivinal
0.203 0.188
92.6
16.06.2016
CMu
RS #2 KBI‐00047 Vivinal
0.203 0.187
92.1
02.06.2016
dc
RS #3 KBI‐00047 Clasado 0.980 0.955
97.4
02.06.2016
dc
RS #3 KBI‐00047 Clasado 0.980 0.937
95.6
07.06.2016
dc
RS #3 KBI‐00047 Clasado 0.980 0.918
93.7
07.06.2016
dc
RS #3 KBI‐00047 Clasado 0.980 0.946
96.5
16.06.2016
CMu
RS #2 KBI‐00047 Clasado 0.980 0.875
89.3
16.06.2016
CMu
RS #2 KBI‐00047 Clasado 0.980 0.873
89.1
02.06.2016
dc
RS #3 KBI‐00047 Vivinal
2.45
2.23
91.0
02.06.2016
dc
RS #3 KBI‐00047 Vivinal
2.45
2.22
90.6
07.06.2016
dc
RS #3 KBI‐00047 Vivinal
2.45
2.26
92.2
07.06.2016
dc
RS #3 KBI‐00047 Vivinal
2.45
2.24
91.4
16.06.2016
CMu
RS #2 KBI‐00047 Vivinal
2.45
2.09
85.3
16.06.2016
CMu
RS #2 KBI‐00047 Vivinal
2.45
2.1
85.7
02.06.2016
dc
RS #3 KBI‐00047 Clasado 4.96
4.83
97.4
02.06.2016
dc
RS #3 KBI‐00047 Clasado 4.96
4.86
98.0
07.06.2016
dc
RS #3 KBI‐00047 Clasado 4.96
4.66
94.0
07.06.2016
dc
RS #3 KBI‐00047 Clasado 4.96
4.64
93.5
16.06.2016
CMu
RS #2 KBI‐00047 Clasado 4.96
4.49
90.5
16.06.2016
CMu
RS #2 KBI‐00047 Clasado 4.96
4.45
89.7
Recovery
97.6
5.0
93.9
3.6
93.6
3.9
89.4
3.4
VALIDATION REPORT
FOR ERP USE ONLY
DO NOT DISTRIBUTE