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Method Performance Feedback 2014.03

GC/MS method. There are, however, 133 pesticides that can be analyzed by GC/MS and 200 by

LC/MS/MS, with LODs ≤10 μg/kg.

Were the method's safety concerns addressed prior to the approval for AOAC First Action Official Methods

status?

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Is the documentation for the safety evaluation available and completed?

No

Yes

No

No

Yes

Yes

Yes

Are there any reference materials considered or addressed?

Yes

No

No

Yes

No

No

No

Is there documentation regarding reference materials available and noted? If so, where is it located?

Chemical and standards are addressed in the method in the appropriate Materials section.

There are no standard reference materials for these pesticide residues.

only documentation regarding preparation of working standards was noted. No information regarding sourcing of

reference materials was made. Also, no information in the study regarding use or results of interlaboratory PT