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Method Performance Feedback 2014.03

reference materials available.(e.g. FAPAS)

I found reference materials (proficiency tests) available from FAPAS. Several of the method users stated there

were reference materials available.

Looking in different databases I could not find information about pesticides in tea reference materials

No data from certified reference materials were presented.

Looking in databases, I could not find information about pesticides in tea reference materials

What type of single laboratory validations were used for this method [i.e, Harmonized PTM, Precollaborative,

Independent, Collaborative, etc.] and where is it referenced in the method documentation?

Independent. See GF Pang's Journal of AOAC publications. One of the publications directly related to the method

is listed as a reference at the end of the official method document.

Pre-collaborative SLV mentioned in the Introduction of the Collaborative Study report/publication

Noted multiple laboratory validations in the Method annex

There was a collaborative study done prior to first action. OMAMAN-14 details the study

The SLV was performed pre-collaborative. Reproducibility was tested by authors using a collaborative study

(MLT).

The information is included in the Method Manuscript.

The method performance was demonstrated in its collaborative study, which was published at J AOAC Int.

Pre-collaborative

Are the approved validation protocols available and documented?

Yes

Yes

No

Yes

Yes

Yes

Yes

Is the method documentation available that demonstrates Reproducibility/Uncertainty and Probability of

Detection? If so, please cite the reference.