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Table 4

Product

SPIFAN Code

Analyte

Nr. replicates (n)

(Duplicates on 3 or

6 days)

Conc. Level

(mcg/100g liquid)

RSDr

b

RSD iR

Conc. Level

RSDr

RSD iR

Child Formula Powder, placebo

00847RF00

Biotin

6

Not detected

NA

NA

(mcg/100g liquid)

≤ Z % ≤ W %

Infant Elemental Powder, Placebo

00796RF00

Biotin

6

Not detected

NA

NA

Biotin

0.1-1

≤ 8

Adult Nutritional RTF High Protein, placebo

00821RF00

Biotin

6

Not detected

NA

NA

Biotin

>1

≤ 6

Adult Nutritional RTF High Fat, placebo

00820RF00

Biotin

6

Not detected

NA

NA

Infant Formula RTF Milk Based, Placebo

EV4H2Q

Biotin

6

Not detected

NA

NA

SRM 1849a

CLC10-b

Biotin

12

22.4

a

1.5

2.6

Infant Formula Powder Partially Hydrolyzed Milk Based

410057652Z

Biotin

12

4.07

0.5

1.6

Infant Formula Powder Partially Hydrolyzed Soy Based

410457651Z

Biotin

12

4.43

0.5

1.3

Toddler Formula Powder Milk-Based

4052755861

Biotin

12

10.7

1.9

4.5

Infant Formula Powder Milk Based

4044755861

Biotin

12

2.90

2.5

3.3

Adult Nutritional Powder Low Fat

00859RF00

Biotin

12

31.9

0.7

2.8

Child Formula Powder

00866RF00

Biotin

12

21.6

1.2

1.8

Infant Elemental Powder

00795RF00

Biotin

12

10.7

1.9

4.5

Infant Formula Powder FOS/GOS Based

50350017W1

Biotin

12

1.66

2.6

4.1

Infant Formula Powder Milk Based

K16NTAV

Biotin

12

5.11

1.2

3.0

Infant Formula Powder Soy Based

E10NWZC

Biotin

12

5.15

3.0

4.0

Infant Formula RTF Milk Based

EV4H2R

Biotin

12

3.86

1.7

4.1

Adult Nutritional RTF High Protein

00730RF00

Biotin

12

56.8

1.0

3.4

Adult Nutritional RTF High Fat

00729RF00

Biotin

12

76.2

0.6

3.1

Global Mean %

1.5

3.2

a. Results reported as mg/kg powder to be consistant with COA.

b. The largest RSDr among the 6 days.

Precision - repeatability.

REQUIREMENTS SMPR

SPIFAN ERP X Checklist v 1.0

Bio-03 (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE