Review Team (February 2016).pdf

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Table 5

System Suitability

SRM Product

Code

Analyte

Reference

value

Sample size

HPLC-Injected

Sample

Measured value

a

Recovery vs CoA

Suitable range

(mg/kg pwd)

(g)

Conc. (ng/mL)

Conc. (mg/kg pwd)

(%)

Level

Conc. (ng/mL)

Conc. (ng/mL)

0.1445

6.276

2.172

109

Blank

0

0.1532

6.981

2.278

114

1

4.981

0.2006

8.454

2.107

106

2

9.962

1.0020

40.21

2.006

101

3

19.92

1.0006

41.05

2.051

103

4

39.85

1.5177

58.69

1.934

97.2

5

59.77

1.5082

57.60

1.910

96.0

6

79.70

2.0006

69.39

1.734

87.1

7

99.62

2.0003

69.28

1.732

87.0

a. Results reported as mg/kg powder to be consistant with COA.

8.45-58.7

Calibration Standard

1849a

CLC-10b

Biotin

1.99

SPIFAN ERP Checklist v1.0

Bio-03 (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE