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Single Laboratory Validation Report for Total Amino Acids by UHPLC-UV in Infant Formulas and Adult Nutritionals
Jaudzems, Lahrichi, and Fuerer
–
January 2017
page 20/20
5
APPENDICES
Appendix A: average values of the SPIFAN II SLV kit products in mg/100 g reconstituted
product.
Appendix B: average values of the SPIFAN II SLV kit products in mg/100 g product.
Appendix C: repeatability performance requirements for each analyte/sample pair
according to the concentration of the analyte in the reconstituted product.
Appendix D: repeatability data obtained with the SPIFAN II SLV kit products, color-coded
with respect to performance requirement values.
Appendix E: reproducibility performance requirements for each analyte/sample pair
according to the concentration of the analyte in the reconstituted product.
Appendix F: intermediate reproducibility data obtained with the SPIFAN II SLV kit products,
color-coded with respect to reproducibility requirement values.
Appendix G: recovery performance requirements for each analyte/sample pair according to
the concentration of the analyte in the reconstituted product.
Appendix H: recovery data obtained with the SPIFAN II SLV kit products, color-coded with
respect to performance requirement values.
Appendix I: example chromatograms for selected concentrations of the calibration curve
and SPIFAN II SLV kit products.
6
REFERENCES
Barkholt V. and Jensen A. L. (1989). Amino acid analysis: Determination of cysteine plus
half-cystine in proteins after hydrochloric acid hydrolysis with a disulphide compound as
additive. Analytical Biochemistry 177, 318-322.
UPLC Amino Acid Analysis Solution System Guide (71500129702 / Revision B). Waters
Corporation, Milford, MA, USA.
AMINO-01 (FEBRUARY 2017)
SLV REPORT
FOR ERP USE ONLY
DO NOT DISTRIBUTE