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Table D: 3M

MDA

Salmonella

Presumptive vs. 3M

MDA

Salmonella

Confirmed – POD Results

Matrix

Analyte

Inoculum Level N

a

Presumptive

Confirmed

dPOD

CP

e

95% CI

f

X

b

POD

CP

c

95% CI

x

POD

CC

d

95% CI

Pasteurized

American

Cheese

Salmonella

enterica ser.

Montevideo

ATCC

g

8387

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

16

0.80

0.58, 0.92

16

0.80

0.58, 0.92

0.00

-0.25, 0.25

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

Concrete

Salmonella

enterica ser.

Enteritidis

ATCC 13076

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

9

0.45

0.26, 0.66

9

0.45

0.26, 0.66

0.00

-0.28, 0.28

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

Creamy

Peanut Butter

Salmonella

enterica ser.

Typhimurium

ATCC 14028

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

10

0.50

0.30, 0.70

10

0.50

0.30, 0.70

0.00

-0.28, 0.28

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

Sprout

Irrigation

Water

Salmonella

enterica ser.

Saintpaul

ATCC 9712

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

10

0.50

0.30, 0.70

10

0.50

0.30, 0.70

0.00

-0.28, 0.28

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

Dry Pet Food

375g

Salmonella

enterica ser.

Poona

NCTC 4840

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

7

0.35

0.18, 0.57

7

0.35

0.18, 0.57

0.00

-0.28, 0.28

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

Ceramic Tile

Salmonella

enterica ser.

Anatum

ATCC 9270

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

10

0.50

0.30, 0.70

10

0.50

0.30, 0.70

0.00

-0.28, 0.28

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

a

N = Number of test portions

b

x = Number of positive test portions

c

POD

CP

=

Candidate method presumptive positive outcomes divided by the total number of trials

d

POD

CC

= Candidate method confirmed positive outcomes divided by the total number of trials

e

dPOD

CP

= Difference between the candidate method presumptive result and candidate method confirmed result POD values

f

95% CI = If the confidence interval of a dPOD does not contain zero, then the difference is statistically significant at the 5% level

g

ATCC = American Type Culture Collection

2013.09 /PTM Matrix Extension Report

March 2014

Expert Review Panel Use Only

AOAC Research Institute

Expert Review Panel Use Only