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Validation

Parameter

Test Group Name

Date

Test Name

Data Path File

Matrix

Raw-Data File Ref.

Limit

CRM Data File Ref.

Equipment

Analyst

Test Method

Operator

Repeatability at LOQ 5 ug/l standard

Sample Blank No.

Mean Retention Time (min)

m/z

Signal (ug/l)

1

2.097

170.2>152.1

5.655

Mean (μg/l)

5.64

2

2.097

170.2>152.1

5.611

SD

0.1082

3

2.097

170.2>152.1

5.723

LOD (Mean +3 sigma)

5.96

4

2.097

170.2>152.1

5.430

LOQ (Mean + 10sigma)

6.72

5

2.097

170.2>152.1

5.788

RSD %

1.92

6

2.097

170.2>152.1

5.548

Standard Conc. (μg/l)

5

7

2.097

170.2>152.1

5.548

Accuracy %

112.7

8

2.097

170.2>152.1

5.614

9

2.097

170.2>152.1

5.749

Accuracy = 70 - 125 %

10

2.097

170.2>152.1

5.685

RSD% = <15%

Page 26

Criteria

Caluclation

Prasad BKVR/Kesav Kumar N

AOAC- SPIFAN-2012-VITAMINS

Limit of Quantification

B-Complex vitamins

pyridoxin

2015\January\Vitamins\01.01.2015

01.01.2015

Aqueous

TUV/BLR/F-360

TUV/BLR/F-99

LC-MS/MS 6460A (BLR/PS-CRS/006.03)

Manjunath K/Prasad BKVR

BVit-03 (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE