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Validation

Parameter

Test Group Name

Date

Test Name

Data Path File

Matrix

Raw-Data File Ref.

Limit

CRM Data File Ref.

Equipment

Analyst

Test Method

Operator

Repeatability at LOQ 5 ug/l standard

Sample Blank No.

Mean Retention Time (min)

m/z

Signal (ug/l)

1

3.941

377.1 >243.2

5.465

Mean (μg/l)

5.35

2

3.941

377.1 >243.2

5.462

SD

0.1195

3

3.941

377.1 >243.2

5.257

LOD (Mean +3 sigma)

5.71

4

3.941

377.1 >243.2

5.358

LOQ (Mean + 10sigma)

6.55

5

3.941

377.1 >243.2

5.192

RSD %

2.23

6

3.941

377.1 >243.2

5.201

Standard Conc. (μg/l)

5

7

3.941

377.1 >243.2

5.439

Accuracy %

107.0

8

3.941

377.1 >243.2

5.537

9

3.941

377.1 >243.2

5.300

Accuracy = 70 - 125 %

10

3.941

377.1 >243.2

5.312

RSD% = <15%

Page 22

Criteria

Caluclation

Prasad BKVR/Kesav Kumar N

AOAC- SPIFAN-2012-VITAMINS

Limit of Quantification

TUV/BLR/F-360

TUV/BLR/F-99

Manjunath K/Prasad BKVR

B-Complex vitamins

Riboflavin

Aqueous

LC-MS/MS 6460A (BLR/PS-CRS/006.03)

01.01.2015

2015\January\Vitamins\01.01.2015

BVit-03 (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE