Review Team (February 2016).pdf

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Validation Parameter
Test Group Name Date 01.01.2015
Test Name Data Path File 2015\January\Vitamins\01.01.2015
Matrix Raw-Data File Ref. TUV/BLR/F-360
Equiment Analyst Manjunath K/Prasad BKVR
With Multilevel Calibration
Calibration Standards Concentration (ug/kg) Area-Analyte
Solvent Standard Level-1 5.00 42920.38
Solvent Standard Level-2 10.00 86685.62
Solvent Standard Level-3 50.00 411233.87
Solvent Standard Level-4 100.00 747190.82
Solvent Standard Level-5 200.00 1356939.66
Solvent Standard Level-6 300.00 1895074.96
Criteria R2 ≥ 0.99
Conclusion Complies
Page 18
LC-MS/MS 6460A (BLR/PS-CRS/006.03)
AOAC- SPIFAN-2012-VITAMINS
Calibration Curve
B-complex Vitamins
Pyridoxin
Aqueous
y = 6283.8x + 60220
R² = 0.9954
0.00
500000.00
1000000.00
1500000.00
2000000.00
2500000.00
0.00 50.00 100.00150.00200.00250.00300.00350.00
BVit-03 (February 2016)
FOR ERP USE ONLY
DO NOT DISTRIBUTE