Review Team (February 2016).pdf

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Validation Parameter
Test Group Name Date 01.01.2015
Test Name Data Path File 2015\January\Vitamins\01.01.2015
Matrix Raw-Data File Ref. TUV/BLR/F-360
Equiment Analyst Manjunath K/Prasad BKVR
With Multilevel Calibration
Calibration Standards Concentration (ug/kg) Area-Analyte
Solvent Standard Level-1 5.00 3037.84
Solvent Standard Level-2 10.00 6191.24
Solvent Standard Level-3 50.00 34554.87
Solvent Standard Level-4 100.00 71591.71
Solvent Standard Level-5 300.00 237068.98
Solvent Standard Level-6 500.00 397766.42
Criteria R2 ≥ 0.99
Conclusion Complies
Page 14
LC-MS/MS 6460A (BLR/PS-CRS/006.03)
AOAC- SPIFAN-2012-VITAMINS
Calibration Curve
B-complex Vitamins
Riboflavin
Aqueous
y = 801.89x - 3934.8
R² = 0.9997
0.00
50000.00
100000.00
150000.00
200000.00
250000.00
300000.00
350000.00
400000.00
450000.00
0.00 100.00 200.00 300.00 400.00 500.00 600.00
BVit-03 (February 2016)
FOR ERP USE ONLY
DO NOT DISTRIBUTE