Review Team (February 2016).pdf

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Validation Parameter
Test Group Name Date 01.01.2015
Test Name Data Path File 2015\January\Vitamins\01.01.2015
Matrix Raw-Data File Ref. TUV/BLR/F-360
Equiment Analyst Manjunath K/Prasad BKVR
With Multilevel Calibration
Calibration Standards Concentration (ug/L) Area-Analyte
Solvent Standard Level-1 5.00 8453.63
Solvent Standard Level-2 20.00 53305.80
Solvent Standard Level-3 100.00 340778.96
Solvent Standard Level-4 200.00 737865.01
Solvent Standard Level-5 300.00 1164641.72
Solvent Standard Level-6 500.00 1891466.35
Criteria R2 ≥ 0.99
Conclusion Complies
Page 13
LC-MS/MS 6460A (BLR/PS-CRS/006.03)
AOAC- SPIFAN-2012-VITAMINS
Calibration Curve
B-complex Vitamins
Thiamine
Aqueous
y = 3850.1x - 22469
R² = 0.9993
-500000.00
0.00
500000.00
1000000.00
1500000.00
2000000.00
0.00 100.00 200.00 300.00 400.00 500.00 600.00
BVit-03 (February 2016)
FOR ERP USE ONLY
DO NOT DISTRIBUTE