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Validation

Parameter

Test Group Name

Date

Test Name

Data Path File

Matrix

Raw-Data File Ref.

Limit

CRM Data File Ref.

Equipment

Analyst

Test Method

Operator

Repeatability at LOQ 5 ug/l standard

Sample Blank No.

Mean Retention Time (min)

m/z

Signal (ug/l)

1

1.867

124.2>80.1

5.617

Mean (μg/l)

5.58

2

1.867

124.2>80.1

5.533

SD

0.3774

3

1.867

124.2>80.1

4.943

LOD (Mean +3 sigma)

6.72

4

1.867

124.2>80.1

5.486

LOQ (Mean + 10sigma)

9.36

5

1.867

124.2>80.1

6.255

RSD %

6.76

6

1.867

124.2>80.1

5.994

Standard Conc. (μg/l)

5

7

1.867

124.2>80.1

5.832

Accuracy %

111.7

8

1.867

124.2>80.1

5.271

9

1.867

124.2>80.1

5.301

Accuracy = 70 - 125 %

10

1.867

124.2>80.1

5.611

RSD% = <15%

Page 24

Criteria

Caluclation

Prasad BKVR/Kesav Kumar N

AOAC- SPIFAN-2012-VITAMINS

Limit of Quantification

B-Complex vitamins

Nicotinic acid

2015\January\Vitamins\01.01.2015

01.01.2015

Aqueous

TUV/BLR/F-360

TUV/BLR/F-99

LC-MS/MS 6460A (BLR/PS-CRS/006.03)

Manjunath K/Prasad BKVR

BVit-03 (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE