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March 2015

AFRICAN FUSION

27

obtained for the interlayer and the 27NiCrMoV base material

respectively. Local maxima were again found in heat affected

zones – the highest in HAZ of 27NiCrMoV base material (up to

350 HV near the face of weldment), lower in the HAZ of the

interlayer (up to 300 HV) and about 320 HV in HAZ of COST F

base material. This means that carbon enrichment increases

hardness, yet the increase is not essential for macroscopic

mechanical properties. The interlayer was again the weakest

part of the weldment.

Dissimilar weld joint D

The last trial weld joint investigated, the weldment of COST

F and COST FB2 steels, was produced in two variants with

different weld metals – Thermanit MTS 3 (D1 weld joint) and

Thermanit MTS 616 (D2 weld joint), which are both based on

modified 9Cr steels. Thermanit MTS 3 contains 1.0 wt.% of

molybdenum, while Thermanit 616 contains 0,4 wt.% of mo-

lybdenum and 1.7 wt% of tungsten. Each variant underwent

three different heat treatment schedules. The best one was

selected on the basis of results of mechanical testing and a

detailed microstructural study was performed using LM, SEM

and TEM. Using that optimised technology a new weld joint

was produced and long term creep testing was carried out.

Results of creep testing together with fractographic analysis

and TEM of carbon replicas and thin foils are summarised in

another paper of this proceedings (Kasl J, Jandov

á

D:Testing

of dissimilar weld joint of steels COST FB2 and COST F).

Microstructures in all zones of theweldment corresponded

to heavy tempered martensite with a high density of precipi-

tates (Figures 13 to 15). The COST F base material unaffected

by welding was significantly coarser than that of FB2. Small

islands of

δ

-ferrite were sporadically observed in the base

materials and more often in the weld metal, especially in the

root. Density of precipitates decreased in the sequence from

FB2 to COST F base materials and then to the weld metal. No

differences between D1 and D2 variants were observable us-

ing LMand SEM. The variant with the weldmetal of Thermanit

616 showed better mechanical properties; therefore this one

underwent additional microstructural study and testing under

creep conditions.

Crossweld hardness profiles of all six variants of weld D

weremeasured (twoweld joints after threemethods of PWHT).

The hardness of the D2 weld after optimal heat treatment

is shown in Figure 16. The hardness of both base materials

unaffected by welding is approximately the same – about

240 HV 10 – and decreased in the HAZ, especially in FB2 steel

to around 200 HV 10. Higher hardness (up to 280 HV 10) was

found in the weld metal. This hardness profile corresponded

to results fromtensile testing. All specimens ruptured in either

the FB2 or COST F base materials.

References

1

Kern TU, Mayer KH, Donth B, Zeiler G, Digianfrancesco

A: The European Efforts in Development of New High

Temperature Rotormaterials – COST536; Proceeding of

the 9

th

Liege Conference, Materials for Advanced Power

Engineering, 2010.

2

J Lecomte-Beckers, Q Contrepois, T Beck, B Kuhn Eds:

Forschungzcentrum J

ü

lich GmbH, Proceeding of the

9

th

Liege Conference, Materials for Advanced Power

Engineering, 2010. pp. 27-36.

Conclusions

Four trial weld joints were investigated. Microstructure was

evaluated using light, scanning and transmission electron

microscopy and thesewere comparedwith results ofmechani-

cal testing. It then became possible to optimise consumables

and PWHT as well as heat treatments of the base materials.

Full conditions of the heat treatments of individual weld joints,

however, cannot be published.

After qualification tests and finalisation of the weld joint

designs, these procedures will be used in real production of

combined rotors for turbines for fossil fuel power plants

Acknowledgements

This work was supported by Grant project TE01020118 from

the Technology Agency of the Czech Republic.

Figure 12: The crossweld hardness profile of Weld C after PWHT.

Figure 13: LM micrograph of Weld D2

showing a martensitic structure in the

COST FB2 base material.

Figure 14: LM micrograph of Weld

D2, which also reveals a martensitic

structure in the COST F base material.

Figure 15: LM micrograph of Weld D2

showing a martensitic structure in the

weld metal.

Figure 16: Crossweld hardness profile of Weld D after optimal PWHT.