Table of Contents Table of Contents
Previous Page  152 / 670 Next Page
Information
Show Menu
Previous Page 152 / 670 Next Page
Page Background

ValidationParameter

TestGroupName

Date

TestName

DataPathFile

Matrix

Raw-DataFileRef.

Equiment

Analyst

SampleBlankNo.

RetentionTime (min)

m/z

Standard (PeakArea)

Blank (PeakArea)

Area%ofblank to

lowestcalibrant

(Criteria=<30%)

Lowestcalibrant

concentrationug/l

1

3.941

377.1 >243.2

4222.7

411.0

9.73

5.0

2

3.941

377.1 >243.2

4220.2

411.0

9.74

5.0

3

3.941

377.1 >243.2

4077.6

411.0

10.08

5.0

4

3.941

377.1 >243.2

4147.9

411.0

9.91

5.0

5

3.941

377.1 >243.2

4032.4

411.0

10.19

5.0

6

3.941

377.1 >243.2

4038.2

411.0

10.18

5.0

7

3.941

377.1 >243.2

4204.4

411.0

9.78

5.0

8

3.941

377.1 >243.2

4272.9

411.0

9.62

5.0

9

3.941

377.1 >243.2

4107.4

411.0

10.01

5.0

10

3.941

377.1 >243.2

4115.9

411.0

9.99

5.0

Mean

3.94

Mean

9.922

Concentration

Analyte Retention

Time (Minutes)

377.1>172.1

Ion Ratio

% Relative

Intensity

RT Difference

(criteria = ± 0.2

minute)

Ion Ratios

Overall

(μg/kg)

Area (Q1)

Area (Q2)

Pass - Fail

Pass - Fail

Calibration standard 1

3.941

4348.308564

2375

0.546

54.6

Pass

Confirmed

Calibration standard 2

3.941

7748.884013

4810

0.621

62.1

Pass

Confirmed

Calibration standard 3

3.941

40826.16555

23723

0.581

58.1

Pass

Confirmed

Calibration standard 4

3.924

82574.58657

48278

0.585

58.5

Pass

Confirmed

Calibration standard 5

3.941

173711.2294

102048

0.587

58.7

Pass

Confirmed

Calibration standard 6

3.941

429749.2638

253557

0.590

59.0

Pass

Confirmed

Mean

3.938

SRM 1849a-1

3.941

88826.34

51682.00

0.58

58

0.003

Pass

Confirmed

SRM 1849a-2

3.924

86761.32

51306.00

0.59

59

-0.015

Pass

Confirmed

SRM 1849a-3

3.923

87018.09

50127.00

0.58

58

-0.015

Pass

Confirmed

SRM 1849a-4

3.941

87652.85

51262.00

0.58

58

0.003

Pass

Confirmed

SRM 1849a-5

3.941

86242.42

51809.00

0.60

60

0.003

Pass

Confirmed

SRM 1849a-6

3.941

87028.15

50820.00

0.58

58

0.003

Pass

Confirmed

Average ion ratio

0.59

Relative intensity (%of

basepeak)

%Toleranceplusorminus

Average intensity

59

>50

30

Tolerance (%)

30.00

>20-50

30

Lower limit

0.41

>10-20

30

Upper limit

0.76

<10

30

Page 6

AOAC-SPIFAN-2012-VITAMINS

MethodBlank

TUV/BLR/F-360

LC-MS/MS

ManjunathK/PrasadBKVR

Specificity

B-ComplexVitamins

01.01.2015

Riboflavin

2015\January\Vitamins\01.01.2015

BVit-03 (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE